Preparation and Characterization of ZnO Nanoparticles Supported on Amorphous SiO2

نویسندگان

  • Ying Chen
  • Hao Ding
  • Sijia Sun
چکیده

In order to reduce the primary particle size of zinc oxide (ZnO) and eliminate the agglomeration phenomenon to form a monodisperse state, Zn2+ was loaded on the surface of amorphous silica (SiO₂) by the hydrogen bond association between hydroxyl groups in the hydrothermal process. After calcining the precursors, dehydration condensation among hydroxyl groups occurred and ZnO nanoparticles supported on amorphous SiO₂ (ZnO-SiO₂) were prepared. Furthermore, the SEM and TEM observations showed that ZnO nanoparticles with a particle size of 3-8 nm were uniformly and dispersedly loaded on the surface of amorphous SiO₂. Compared with pure ZnO, ZnO-SiO₂ showed a much better antibacterial performance in the minimum inhibitory concentration (MIC) test and the antibacterial properties of the paint adding ZnO-SiO₂ composite.

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

منابع مشابه

Sol-gel Synthesis of ZnO Nanoparticles and ZnO-TiO2-SiO2 Nanocomposites and Their Photo-catalyst Investigation in Methylene Blue Degradation

In this work firstly ZnO nanoparticles were synthesized via a simple precipitation method. At the second step titanium dioxide and silicon dioxide shell were synthesized on the core. For preparation ZnO-TiO2-SiO2 the sol product was calcinated at 500 ºC for 2h. Properties of the product were examined by X-raydiffraction pattern (XRD), scanning electron microscope (SEM) and Fourier transform inf...

متن کامل

Synthesis, Characterization and Catalytic Performance in the Selective Oxidation of Alcohols by Metallophthalocyanines Supported on Zinc Oxide Nanoparticles

Unsubstituted phthalocyanines of Co, Fe and Mn supported on zinc oxide nanoparticles were prepared and were well characterized with X-ray diffraction and scanning electron microscopy. The oxidation of alcohols with tert-butylhydroperoxide, in the presence of metallophthalocyanines supported on zinc oxide nanoparticles was investigated. These MPc/ZnO nanocomposites were effective catalysts for t...

متن کامل

SiO2/ZnO Composite Hollow Sub-Micron Fibers: Fabrication from Facile Single Capillary Electrospinning and Their Photoluminescence Properties

In this work, SiO2/ZnO composite hollow sub-micron fibers were fabricated by a facile single capillary electrospinning technique followed by calcination, using tetraethyl orthosilicate (TEOS), polyvinylpyrrolidone (PVP) and ZnO nanoparticles as raw materials. The characterization results of the scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffraction (XRD) a...

متن کامل

Preparation, Characterization, and Application of Nanospherical α-Fe2O3 Supported on Silica for Photocatalytic Degradation of Methylene Blue

In the research, spherical α-Fe2O3 NanoParticles (NPs) were synthesized through Forced Hydrolysis and Reflux Condensation (FHRC) process and were supported on the surface of silica sand by Solid-State Dispersion (SSD) method. Characterization of silica and α-Fe2O3/SiO2 catalyst was done using Fourier-Transform InfraRed (FT-IR) spectrosc...

متن کامل

FTIR and Raman Spectroscopy of Carbon Nanoparticles in SiO2, ZnO and NiO Matrices

Coatings of carbon nanoparticles dispersed in SiO2, ZnO and NiO matrices on aluminium substrates have been fabricated by a sol–gel technique. Spectrophotometry was used to determine the solar absorptance and the thermal emittance of the composite coatings with a view to apply these as selective solar absorber surfaces in solar thermal collectors. Cross-sectional high resolution transmission ele...

متن کامل

ذخیره در منابع من


  با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

عنوان ژورنال:

دوره 7  شماره 

صفحات  -

تاریخ انتشار 2017